Planetary Ball Mill PM 200

Артикул: PM 200

The Planetary Ball Mill PM 200 is a powerful benchtop model with 2 grinding stations for grinding jars with a nominal volume of 12 ml to 125 ml.

The extremely high centrifugal forces of Planetary Ball Mills result in very high pulverization energy and therefore short grinding times.
The PM 200 can be found in virtually all industries where the quality control process places the highest demands on purity, speed, fineness and reproducibility.
The mill is ideally suited for tasks in research like mechanochemistry (mechano-synthesis, mechanical alloying and mechanocatalysis), or ultrafine colloidal grinding on a nanometer scale, as well as for routine tasks such as mixing and homogenizing soft, hard, brittle or fibrous materials.

TWO GRINDING STATIONS FOR STANDARD APPLICATIONS

    • Max. speed 650 rpm
    • Up to 10 mm feed size and 0.1 µm final fineness
    • 2 grinding stations for jars from 12 ml up to 125 ml, jars of 12 and 25 ml can be stacked (two jars each)
    • GrindControl to measure temperature and pressure inside the jar.
    • Aeriation lids to control the atmosphere inside the jar
    • Storable SOPs and cycle programs, 5 different jar materials for dry and wet grinding

    FAST & POWERFUL

    • Loss-free size reduction down to the submicron range
    • Wet grinding yields particle sizes in the nanometer range (<100 nm)
    • Variable speed from 100 to 650 rpm,
    • speed ratio 1:-2
    • Grinding with up to 33.3 x acceleration of gravity
    • Batch-wise processing with max. 2 x 50 ml sample
    • Wide range of materials for contamination free grinding

    REPRODUCIBILITY, SAFETY AND EASY HANDLING

    • Reproducible results due to speed control
    • Easy and safe clamping of grinding jars
    • The Safety Slider prevents starting the machine without securely clamped jars
    • Perfect stability on the lab bench thanks to FFCS technology
    • Innovative counterweight and imbalance sensor for unsupervised operation
    • Comfortable parameter setting via display and ergonomic 1-button operation
    • Automatic grinding chamber ventilation
    • 10 SOPs can be stored, programmable starting time
    • Power failure backup ensures storage of remaining processing time

    SETTINGS & OPTIONS

    • Dry and wet grinding possible
    • Suitable for long-term trials, 99 h max.
    • Interval operation allows for cooling breaks
    • Direction reversal helps to minimize caking effects

    WET AND NANO-SCALE GRINDING WITH THE PM 200

    Wet grinding is used to obtain particle sizes below 5 µm, as small particles tend to get charged on their surfaces and agglomerate, which makes further grinding in dry mode difficult. By adding a liquid or dispersant the particles can be kept separated.

    To produce very fine particles of 100 nm or less (nano-scale grinding) by wet grinding, friction rather than impact is required. This is achieved by using a large number of small grinding balls which have a large surface and many friction points. The ideal filling level of the jar should consist of 60 % small grinding balls.
    For more details on jar filling, wet grinding and sample recovery watch the video.

    The graphic shows the result of grinding barium titanate at 500 rpm in the PM 200. After 5 h of pulverization in heptane and oleic acid mixture with 0.5 mm grinding balls, the D90 value of the original sample was reduced from 15 µm to 95 nm.

     

    Grinding of barium titanate in heptane and oleic acid mixture with 0.5 mm grinding balls.

    Blue curve: original sample; green curve: pulverized sample after 5 h. 

    TYPICAL SAMPLE MATERIALS

    RETSCH planetary ball mills are perfectly suitable for size reduction of, for example, alloys, bentonite, bones, carbon fibres, catalysts, cellulose, cement clinker, ceramics, charcoal, chemical products, clay minerals, coal, coke, compost, concrete, electronic scrap, fibres, glass, gypsum, hair, hydroxyapatite, iron ore, kaolin, limestone, metal oxides, minerals, ores, paints and lacquers, paper, pigments, plant materials, polymers, quartz, seeds, semi-precious stones, sewage sludge, slag, soils, tissue, tobacco, waste samples, wood, etc.

    Medium-hard: biomass
    35 g sample
    125 ml stainless steel grinding jars
    7 x 20 mm stainless steel grinding balls
    15 min at 500 rpm
    Brittle: tin sulfide
    52 g sample
    125 ml agate grinding jars
    50 x 10 mm agate grinding balls
    60 min at 550 rpm
    10 min intervals and direction reversal
    Fibrous: straw
    7 g sample
    125 ml zirconium oxide grinding jars
    50 x 10 mm zirconium oxide grinding balls
    40 min at 300 rpm
    10 min intervals and direction reversal

    Hard: natural rocks
    60 g sample
    125 ml stainless steel grinding jars
    7 x 20 mm stainless steel grinding balls
    10 min at 420 rpm

    TECHNICAL DATA

    Applicationspulverizing, mixing, homogenizing, colloidal milling, mechanical alloying, mechanosynthesis, nano grinding
    Field of application agriculture, biology, chemistry, construction materials, engineering / electronics, environment / recycling, geology / metallurgy, glass / ceramics, medicine / pharmaceuticals
    Feed material soft, hard, brittle, fibrous - dry or wet
    Size reduction principle impact, friction
    Material feed size*  < 4 mm
    Final fineness*  < 1 µm, for colloidal grinding < 0.1 µm
    Batch size / feed quantity* max. 2 x 50 ml
    No. of grinding stations 2
    Speed ratio 1 : -2
    Sun wheel speed 100 - 650 min-1
    Effective sun wheel diameter 157 mm
    G-force 37,1 g
    Type of grinding jars  EasyFit, optional areation covers, safety closure devices
    Material of grinding tools  hardened steel, stainless steel, tungsten carbide, agate, sintered aluminum oxide, silicon nitride, zirconium oxide
    Grinding jar sizes  12 ml / 25 ml / 50 ml / 80 ml / 125 ml
    Stackable grinding jars  12 ml / 25 ml 
    Setting of grinding time digital, 00:00:01 to 99:59:59
    Interval operation yes, with direction reversal
    Interval time 00:00:01 to 99:59:59
    Pause time 00:00:01 to 99:59:59
    Storable SOPs 10
    Measurement of input energy possible yes
    Interface RS 232 / RS 485
    Drive 3-phase asynchronous motor with frequency converter
    Drive power 750 W
    Electrical supply data different voltages
    Power connection 1-phase
    Protection code IP 30
    Power consumption ~ 1250 W (VA)
    W x H x D closed 640 x 480 (780) x 420 mm
    Net weight ~ 76 kg
    StandardsCE
    Patent / Utility patent 

    SafetySlider (DE 202008008473)

    *depending on feed material and instrument configuration/settings

    FUNCTIONAL PRINCIPLE

    The grinding jars are arranged eccentrically on the sun wheel of the planetary ball mill. The direction of movement of the sun wheel is opposite to that of the grinding jars in the ratio 1:-2.The grinding balls in the grinding jars are subjected to superimposed rotational movements, the so-called Coriolis forces.
    The difference in speeds between the balls and grinding jars produces an interaction between frictional and impact forces, which releases high dynamic energies. The interplay between these forces produces the high and very effective degree of size reduction of the planetary ball mill.